
XRF / XRD Item Code: 99-0501-00
Consists of the following:
· 3 kW X-ray generator, 60 kV, high frequency, air cooled, stability .005% for full rated mains variation, ripple 0.03% to 0.75%. Temp. coeff. 50 ppm/deg. C.
· Goniometer, 2 independent axes, radius 180-250 mm, 0.002 deg minimum step size, <0.0001 deg resolution. Range –12 to +160° 2Theta depending on accessories.
· Detector arm with a curved graphite monochromator and Xe proportional detector Part No. 95-0655-00.
· Tube Shield with shutter under software control.
· XRD tube (Cu) Part No. 97-2673-00 and HT cable. Water is needed for tube cooling only and requirement is 4 litre/min at 15–20°C.
· Cabinets are in vertical configuration 1100 mm wide x 700 mm deep x 900 mm high. The beam-path is surrounded by 2 mm steel and 12 mm Pb-Acrylic (0.5 mm Pb-equivalent). Elsewhere 2 mm aluminium is used for reduced weight and portability.
· An optional floor-standing cabinet is available (not included).
· An integrated Fail-Safe X-rays-on warning lamp is included.
· Microprocessor controller with counting electronics is included. Scan speeds 0.14 deg/min to 100 deg/min. With Multi-pass Averaging, scan speeds 1000 x slower. Slew speed 300 deg/min.
· Software – VisualXRD and Tracesv6 included – 32 bit software for Microsoft Windows operating system.
VisualXRD Software Specifications
· 32 bit application for operation of the EMMA and collection of data files for analysis by Tracesv6 or other applications.
· Simple routine operation enter Start, End angles, Step size, Scan speed, Comment and click start button.
· File Save and recall Parameter sets.
· Software configuration for user Folder, Screen options.
· Hardware configuration for Tube Anode selection and Communications.
· Accessory configuration to select interchangeable options, Source, Optic, Stage, Detector, which each have their own Calibration angles.
· Manual control for computer-aided alignment, move axes anywhere, load sample open/close shutter, start/stop spinner – depending on options installed.
· Pulse Height Analysis used with Xe proportional detector, does a PHA scan, set Lower and upper discriminator, Amp. Gain, Detector HV.
· Data collection modes – Single pass, Multi pass, multi range, Theta/2Theta, Theta only, 2Theta only, Continuous scan, Residual Stress.
Tracesv6 Software Specifications. Part No 95-0573-00
Traces V6.7: 32 bit XRD Scan Processing for Microsoft Windows™ operating system
· Process scans from Diffraction Technology, Siemens, Philips and Rigaku systems
· Tool buttons with tool tips and menus make the software very user-friendly
· Zooming, scrolling and on-screen graphical peak labeling
· 16 million colours with graphical selection
· Work with up to 50 scans on screen at once
· 3D Graphics – perspective, trend lines, surface, tape, area, rotation, colour, printing
· Attribute-based file finder for multi user environments
· Automatic and manual background fit & strip (fitting cubic or linear functions)
· Save scans in a number of formats, or cut and paste to other applications
· Automatic peak search and edit
· Scan manipulation , add, subtract, trim, and spike removal
· Smoothing, cubic, with no loss of high frequency data
· Ka2 stripping
· Peak area, Peak area based quantitation
· Logarithmic vertical scale, toggle on/off
· Peak FWHM determined graphically
· Particle Size by Scherrer method
· Retrieval of PDF1,2 and 4 records displayed as line markers on the screen
· Print preview mode with 2D and 3D scan display. Up to 50 scans in Isometric mode with hidden-line removal for best presentation
· Print PDF Cards from PDF-2 and PDF-4
· Line widths and line-styles selectable
· Powder Pattern Generator with user data or ICDD data
· Peak fitting and deconvolution – large no. of peaks, Least Squares or Genetic algorithm
· Full Windows HELP system and manual included
· Main screen offsets for multiple scan display
· Printing – allows PDF-stick figures and labels on isometric display
· Common functions accessed by right mouse button click
· Angled label text for clearer presentation
· Retained Austenite coupled with VisXRD data collection
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Standard accessories kit with sample holders, slits and alignment tools. |
Included free of charge |
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Water Circulator Unit 220/240 V, 50 Hz. Part No. 96-0101-00 |
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Specifications:
Nominal cooling capacity: 2,600W (25°C)
Output temperature range: 5 ~ 35°C
Temperature accuracy: ± 0.1°C
Tank size: 26 L
Output pressure: 0.57 MPa
Output flow: 6 L/min
Filtration: 10 μm
Power consumption: 1 kW
Weight: 84 kg
Noise: 45 dB
Size (W × D × H): 490 × 580 × 820 mm
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XRD Match Software with Crystallography Open Database – single license. Part No. 31-0511-00 |
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